Short Path Distillation Machine
Example: The specification list of distillation for CBD
(1) Laboratory Test (<20L)
NCF-10A, NCF-20A, NCF-30A, NCF-50A
(2) Pilot Production (20L<100L)
NCF-100, NCF-200
(3) Industrial Production (100L<300L)
NCF-500
2. Customization
The details pls download The Request List of Short Path Distillation
(1)Design support
(2) Directly supply the Senior R&D organic intermediate, shorten your R&D time and cost
(3) Share the advanced purifying technology with you
(4) Supply the high quality chemicals and analysis reagent
(5) We want to assist you on Chemical Engineering (Auto CAD, Aspen plus etc.)
3. Assurance
(1) CE and ISO certification Registered
(2) Trademark: ACHIEVE CHEM(since 2008)
(3) Replacement parts within 1-year for free
Description
Technical Parameters
The operation process of the short path distillation machine is that the steam generated after the mixed liquid boils enters the fractionation column, where it is partially condensed, and the condensate contacts with the rising steam on the way down, and the two exchange heat, so that the high-boiling components in the steam are condensed, while the low-boiling components in the condensate still rise as steam, while the low-boiling components in the condensate are heated and gasified, and the high-boiling components still fall as liquid.
This process is repeated repeatedly, which is equivalent to ordinary distillation for many times in a row. As a result, the low-boiling components in the rising steam increase, and the high-boiling components in the falling condensate increase. In this way, after many times of heat exchange, the separation of high boiling point components and low boiling point components is realized.
We provide short path distillation machine, please refer to the following website for detailed specifications and product information.
Product: https://www.achievechem.com/chemical-equipment/short-path-distillation-machine.html
Product Introduction
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Distillation machine is suitable for all kinds of materials, including materials with high boiling point, heat sensitivity, easy oxidation and emulsification. In specific use, different scraper forms need to be selected according to the characteristics of materials. For example, for materials with high viscosity and high surface tension, spiral scraper or flat scraper can be selected; For materials with low viscosity and low surface tension, you can choose a circular scraper. When using the short path distillation machine, it is necessary to check whether the inlet and outlet valves of the cooling fluid of each component are in the open state, to avoid scalding caused by excessive surface temperature of the external heating body of the equipment, to ensure that the ethanol in the low-temperature thermostatic bath is sufficient, to pay attention to whether the liquid nitrogen in the cold trap is sufficient, and to check whether the connection between the cold trap and the equipment is airtight. |
In addition to short-path distillation, there are the following common separation technologies:
◆ Distillation: The method and process of separating components in liquid mixture by using their volatility.
◆ Sublimation method: the phenomenon that a solid substance is directly transformed into a gas state without being in a liquid state, which can be used as a method for separation by using solid-gas equilibrium.
◆ Crystallization separation method: The solubility of solid in solvent generally increases with the increase of temperature. If the solid is dissolved in a higher temperature solvent to reach saturation, after cooling, the solution will become supersaturated due to the decrease of solubility, and crystals will be precipitated.
◆ Salting-out method: A small amount of salt (such as ammonium sulfate, sodium sulfate, ammonium chloride, etc.) can promote the dissolution of protein. When the salt solution added to protein reaches a certain concentration, the solubility of protein is reduced and precipitated from the solution.
◆ Precipitation separation method: The sample components are precipitated by chemical reaction to form precipitation or adding precipitant to destroy the stability of colloidal solution, and then the precipitated components are obtained (or discarded) by filtration or centrifugation.
◆ Extraction separation method: Liposoluble molecules are extracted with organic solvent and then volatilized to remove the solvent.
◆ Chromatographic separation method: when the sample flows through the chromatographic column, the components are separated one by one because of the different residence time on the column for physical and chemical reasons.
◆ Electrophoretic separation method: This is established according to the phenomenon that the particles with points move towards the opposite electrode under the action of electric field.
◆ Centrifugal separation plate method: It is a method to separate substances under the action of centrifugal force by using the sedimentation coefficient difference of colloidal solute.
Product classifications

Product Features
In short range distillers, the scraper separation device is a key component, especially in rotary scraper short range distillers. The main function of this device is to increase the mass transfer area by scraping the thin layer of liquid, while maintaining the uniformity and stability of the liquid film through rotation, thereby improving the separation effect.
Specifically, the scraper separation device consists of a series of scrapers installed on a rotating shaft. When the rotating axis begins to rotate, the scraper will continuously scrape the thin layer of liquid inside the still. This process not only increases the contact area between the liquid and the wall of the still, thereby improving mass transfer efficiency, but also maintains uniformity and stability of the liquid film through the movement of the scraper.
The scraper separation device in short path distillation machine is a common separation device, which can realize efficient and accurate separation process. A separation device in the form of a scraper usually consists of the following parts:
Scraper
Used to evenly distribute and push the liquid mixture in the evaporation chamber. Scrapers are usually made of stainless steel or other corrosion-resistant materials, which have good corrosion resistance and wear resistance.
Separation column
To separate the liquid mixture into different components. The separation column is usually made of stainless steel or glass, and its internal surface is smooth to reduce the residence time and adhesion of the mixture in the separation column.
Baffle
It controls the flow speed and direction of liquid mixture to improve separation efficiency. The baffle is usually made of stainless steel or plastic and can be adjusted and replaced as needed.
Analysis of advantages and disadvantages
Advantages
◆ Efficient separation: Short-range distillation machines can achieve efficient separation of components in the mixture, especially for components with similar boiling points or similar physical properties, the separation effect is better.
◆ Low temperature operation: Due to the high vacuum, the short-range distillation machine can operate at a lower temperature, avoiding the damage of high temperature to heat-sensitive substances, maintaining the purity and quality of the separated substances.
◆ Energy saving and environmental protection: The short-range distillation machine can achieve low temperature distillation in the distillation process, reducing energy consumption, while reducing waste gas and wastewater discharge, in line with the requirements of sustainable development.
◆ Strong flexibility: The short-range distillation machine can adjust the heating temperature, system pressure and condensing surface distance according to different material characteristics and separation requirements to achieve the best separation effect.
Disadvantages
◆ High equipment cost: The structure of the short-range distillation machine is complex, the material sealing requirements are high, and the distance between the evaporation surface and the condensing surface should be moderate, resulting in greater difficulty in equipment processing and higher cost.
◆ Operation is relatively difficult: the operation of short-range distillation machines requires a certain amount of professional knowledge and experience, and operators need to understand the working principle and operation process of the equipment to ensure the normal operation of the equipment and the accuracy of the experimental results.
Applications
Short-range molecular distillation is a technology to control the molecular spacing in liquid crystal materials by changing the solvent temperature, which is widely used in the design and preparation of functional liquid crystal materials. In the field of liquid crystal display, short distance molecular distillation can be used to adjust the arrangement of liquid crystal molecules, so as to achieve better display effect. In addition, short-range molecular distillation can also be applied to the following aspects:
◆ Optical materials: Molecular distillation can be used to prepare liquid crystal materials with specific structures and optical properties, for example, liquid crystal materials with high refractive index, dispersion performance and noise reduction performance.
◆ Sensor: Using the control ability of short path distillation machine to liquid crystal materials, a liquid crystal sensor with fast response time and good stability can be manufactured to detect environmental parameters such as temperature, pressure and humidity.
◆ Biomedicine: After distillation, liquid crystal materials can be used in biomedical field, for example, for preparing liquid crystal materials with specific structure and biological affinity, and for the research of anti-tumor drugs and medical imaging.
◆ Organic electronics: Molecular distillation system can be used to prepare liquid crystal materials with excellent electrical properties, which is widely used in the field of flexible organic electronics.
Conclusion and prospect
As an advanced separation technology, short-range distillation machine plays an important role in many fields by virtue of its remarkable advantages of high efficiency, energy saving and environmental protection. With the progress and development of science and technology, short-range distillation machines are expected to be improved and innovative in materials, structure, function and other aspects to adapt to a wider range of application needs. For example, the development of new short-range distillation machines with higher separation efficiency, lower energy consumption and greater stability; The intelligent short-range distillation machine with intelligent control, remote monitoring and data analysis is developed. These improvements and innovations will further improve the performance and efficiency of short-range distillation machines, providing more convenient and efficient solutions for research and production.
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