Electric Heating Reactor
(1)2L/3L/5L/10L/20L/30L/50L/100L/150L/200L---Standard
(2)2L/3L/5L/10L/20L/30L/50L/100L/150L/200L---EX-proof
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Description
Technical Parameters
Electric heating reactor is a kind of chemical reaction equipment which uses electric energy to heat the reaction system to a certain temperature. By converting electric energy into heat energy, it makes the reactants in the reaction kettle reach a specific temperature condition, thus promoting the chemical reaction.
Heating reactor usually includes reaction kettle, heater, temperature control device, stirring device and other components to meet the requirements of different reaction systems. It is widely used in various chemical synthesis, organic synthesis, catalytic reaction, material preparation, biotechnology and other fields, and provides an important tool and means for achieving efficient, accurate and safe reactions.
Product Introduction
The working principle of electric heating reactor is to convert electric energy into heat energy, so that the reactants in the reactor can reach the required temperature. In general, the reaction kettle is made of high-temperature resistant materials and has good heat resistance. The heater is usually an electric heater or an electric heating rod placed outside the reaction kettle, which flows into the heater through electric current to generate heat and conduct it to the reaction kettle, thus heating the reaction system.
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In order to accurately control the reaction temperature, heating reactors equipment are usually equipped with temperature control equipment, such as temperature sensors and PID controllers. The temperature sensor can monitor the temperature of the reaction system in real time, and convert the temperature signal into an electrical signal and transmit it to the PID controller. The PID controller compares the set temperature value with the actual measured value, and adjusts the current output to control the power of the heater, thus keeping the reaction temperature stable.
In addition to heating equipment and temperature control equipment, reactors usually include auxiliary equipment such as agitator, feed inlet and exhaust device. The agitator can evenly mix the reactants to improve the reaction efficiency; The feed inlet is used for adding reactants or solvents; The exhaust device is used to exhaust the gas generated by the reaction. |
Product Features
In the electric heating reactor, the common electrode types include the following:
◆ Metal electrode: Metal electrode is one of the most common electrode types. Commonly used metal electrode materials include stainless steel, titanium, nickel, copper and so on. Metal electrodes have good electrical conductivity and corrosion resistance, and are suitable for most electric heating reactors.
◆ Carbon electrode: Carbon electrode is made of carbon materials, such as graphite, graphitized silicon, graphitized carbon, etc. Carbon electrode has good electrical conductivity and high temperature resistance, and is suitable for high temperature reaction.
◆ Oxide electrode: Oxide electrode is usually made of metal oxide or semiconductor material, such as aluminum oxide (Al2O3), titanium dioxide (TiO2) and so on. Oxide electrode has high corrosion resistance and stability, and is suitable for some special reaction conditions.
◆ Alloy electrode: Alloy electrode is a material composed of two or more metals. Alloy electrodes can combine the advantages of different metals to provide better electrical conductivity and corrosion resistance.
◆ Coated electrode: Coated electrode is the coating of corrosion-resistant material or conductive material applied to the basic metal electrode. The coating layer is usually composed of ceramics, metal oxides and other materials to provide better corrosion resistance and stability.
Product Knowledge
Electric heating stainless steel reactor and electric heating homogenizer are two common chemical reaction equipment, and there are some differences in their design and function.
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◆ Design structure: Electric heating stainless steel reactor usually adopts cylindrical or cylindrical structure, with a reaction kettle and heater. It is mainly used to heat the reaction system to a certain temperature to promote the chemical reaction. However, electric heating homogenizers are mostly closed containers with high-speed rotating blades, stirrers or homogenizing devices. Through shearing, extrusion and impact, the reactants are evenly mixed and homogenized under high shear.
◆ Application: Electric heating stainless steel reactor is mainly used in chemical synthesis, organic synthesis, catalytic reaction, material preparation and other fields that need to control the reaction temperature. It is suitable for large-scale production and can carry out continuous or intermittent reaction. Electric heating homogenizer is widely used in food, medicine, cosmetics and other industries, which plays the role of uniform mixing and particle size regulation in the process of preparing emulsion, emulsion, suspension and lactic acid bacteria fermentation.
◆ Reaction mode: Electric heating stainless steel reactor generally adopts batch or continuous reaction mode, which can control parameters such as temperature, time and reactant addition, and is suitable for all kinds of complex chemical reactions. The electric heating homogenizer mainly homogenizes the reaction system by stirring and high-speed shearing force, and usually completes the reaction process in a short time.
◆ Features of the equipment: The electric heating stainless steel reactor has the advantages of accurate temperature control, fast heating speed and large reaction capacity, and is suitable for long-term reaction process. The electric heating homogenizer has the characteristics of good stirring and mixing effect, adjustable homogenization effect and high production efficiency, and is suitable for reaction systems requiring high homogenization.
Cases
In the synthesis of carboxylic acid derivatives, electric heating reactor is usually used for anhydride synthesis and esterification. The following are the chemical principles of these two reactions:
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◆ Anhydride synthesis: Anhydride is an acyl compound generated by dehydration reaction of corresponding carboxylic acid. In SS reactor, an anhydrizing agent (such as acetic anhydride) is usually used to react with carboxylic acid to generate anhydride. In the reaction mechanism, the acetate ion in the anhydride agent acts as a nucleophile, attacking the carbonyl carbon of the carboxyl group, forming a five-membered ring transition state, then breaking and removing a water molecule, and finally generating the anhydride product.
◆ Esterification reaction: Esters are ester-based compounds generated by the reaction of carboxylic acids with alcohols. In the reactor, the reactants carboxylic acid and alcohol are usually used to carry out esterification under certain reaction conditions. In the reaction mechanism, the carbonyl carbon of carboxylic acid has strong electrophilicity and is easily attacked by nucleophilic reagents of alcohol to form an acyloxy compound, and then ester products are finally generated through proton transfer and removal of water molecules. |
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