Horizontal Tube Furnace
2.Lab Box Furnace Equipment:1L-36L
3.Working Temperature can reach 1200℃-1700℃
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Description
Technical Parameters
Introduction to Horizontal Tube Furnace,it is a heating equipment widely used in materials science, chemical engineering, semiconductor manufacturing and other fields. Its structural feature lies in the horizontal arrangement of furnace tubes, which are heated by heating elements to treat the materials inside the furnace tubes. It heats the sample through horizontally arranged furnace tubes, which has the advantages of precise temperature control, uniform heating, and easy operation.
Especially in semiconductor manufacturing, it has a wide range of applications and significant value. Its unique structure and function make it highly valuable in applications such as silicon wafer annealing, heat treatment, metallization process, etching process, and packaging process. At the same time, the high-precision control, high-efficiency processing, good adaptability, and excellent stability of the it also make it highly reliable and stable in semiconductor manufacturing.



Parameter


Working principle
The working principle of a horizontal tube furnace is based on the principles of heat conduction and convection. When the heating element is powered on for heating, heat is transferred to the furnace tube and sample through thermal conduction, while the hot air inside the furnace evenly distributes the heat throughout the entire furnace through convection.
Heating process:
After the heating element is powered on, it generates heat and transfers it to the furnace tube. After the furnace tube is heated, it transfers heat to the sample inside. Due to the excellent thermal conductivity of the furnace tube, the sample can quickly reach the set temperature.
Temperature control:
The temperature control system monitors the temperature inside the furnace in real time and adjusts the power of the heating element based on the difference between the set temperature and the measured temperature. When the measured temperature is higher than the set temperature, the controller reduces the power of the heating element; When the measured temperature is lower than the set temperature, the controller increases the power of the heating element. By continuously adjusting the power of the heating element, the temperature inside the furnace can be maintained constant.
Atmosphere control:
The atmosphere control system controls the atmosphere environment inside the furnace by adjusting the gas flow rate and type. For example, in the semiconductor manufacturing process, it is necessary to control the oxygen and water vapor content inside the furnace to avoid sample oxidation and contamination. The atmosphere control system can accurately control the atmosphere environment inside the furnace to meet the process requirements.
The specific application of horizontal tube furnce in semiconductor manufacturing
The horizntal tube furnce has a wide range of applications in semiconductor manufacturing, and its unique structure and function make it one of the indispensable equipment in the semiconductor processing process.
Basic structure and working principle
A horizntal tube furnce is a commonly used semiconductor processing equipment, which looks like a long tube and has a high-temperature reaction chamber inside. The device adopts an atmosphere control method, and different atmosphere environments can be selected according to different processing requirements to achieve the best processing effect.
The working principle of a horiontal tube furnce is to heat the reactants inside the furnace cavity, causing them to undergo chemical reactions or physical changes at high temperatures, thereby achieving the purpose of processing. In semiconductor manufacturing, horizontal tube furnces are mainly used for annealing and heat treatment of silicon wafers.
Application in silicon wafer annealing
Improve the integrity of silicon wafer lattice
Silicon wafer is one of the important materials in the semiconductor industry, and its quality and performance directly affect the reliability and performance of semiconductor devices. During the processing, silicon wafers are prone to grain boundary stretching due to stress, which can lead to the fracture and damage of silicon crystals. Through high-temperature annealing in a horiontal tube furnace, stress in the silicon wafer can be removed, keeping it intact and avoiding damage to the silicon wafer lattice.
During the annealing process, the silicon wafer is placed inside a horiontal tube furnace and kept at high temperature for a period of time, gradually releasing the internal stress of the silicon wafer and rearranging the lattice, thereby improving the lattice integrity of the silicon wafer.
Improving the electrical properties of silicon wafers
The electrical properties of silicon wafers are one of the key factors affecting the performance of semiconductor devices. By annealing in a horiontal tube furnace, the electrical properties of silicon wafers can be improved, and their conductivity and stability can be enhanced.
During the annealing process, the silicon wafer reacts with the atmosphere inside the furnace at high temperatures, removing the oxide on the surface of the silicon wafer and activating the impurity atoms inside the silicon wafer, thereby improving its electrical properties.
Removing oxides from the surface of silicon wafers
The surface of silicon wafers often contains oxides, which can affect their conductivity and stability. During the manufacturing process, it is necessary to remove oxides from the surface of silicon wafers to ensure their flatness and smoothness, thereby improving the performance of semiconductor devices.
The horiontal tube furnace can remove oxides on the surface of silicon wafers through atmosphere control. During the annealing process, the atmosphere inside the furnace reacts with the oxide on the surface of the silicon wafer to generate volatile substances, which are then discharged through the exhaust system of the furnace to achieve the goal of removing the oxide.
Application in silicon wafer heat treatment
Control of doped silicon wafers
In semiconductor devices, silicon wafers doped with different materials are required due to varying electrical performance requirements. The horiontal tube furnace can use different atmosphere control parameters to control the degree and depth of doping of silicon wafers, in order to meet the requirements of different devices for silicon wafer doping.
During the doping process, the silicon wafer is placed inside a horiontal tube furnace, and the atmosphere inside the furnace reacts with the silicon wafer, allowing the doped atoms to enter the interior of the silicon wafer. By adjusting parameters such as atmosphere and temperature inside the furnace, the number and distribution of doped atoms can be controlled to achieve the desired doping effect.
Preparation of Thin Films on Silicon Wafer Surface
In semiconductor manufacturing, it is sometimes necessary to prepare a thin film on the surface of a silicon wafer to improve its performance or achieve specific functions. A horizntal tube furnace can be used for thin film preparation on the surface of silicon wafers.
During the thin film preparation process, the silicon wafer is placed inside a horizontal tube frnace, and the atmosphere inside the furnace reacts with the surface of the silicon wafer at high temperatures to generate the desired thin film. By adjusting parameters such as atmosphere, temperature, and reaction time inside the furnace, the thickness, composition, and properties of the film can be controlled.
Oxidation and Nitriding of Silicon Wafers
The oxidation and nitridation of silicon wafers are important process steps in semiconductor manufacturing. Horizntal tube furnace can be used for oxidation and nitriding treatment of silicon wafers.
During the oxidation process, the silicon wafer is placed in the furnace chamber of a horizntal tube furnace, and the oxygen in the furnace chamber reacts with the surface of the silicon wafer at high temperature to form a silicon dioxide film. By adjusting parameters such as oxygen concentration, temperature, and reaction time inside the furnace, the thickness and properties of the silicon dioxide film can be controlled.
During the nitriding process, the silicon wafer is placed inside a horizntal tube furnace, and the nitrogen gas inside the furnace reacts with the surface of the silicon wafer at high temperatures to form a silicon nitride film. Silicon nitride thin films have excellent wear resistance, corrosion resistance, and high-temperature stability, which can be used to protect the surface of silicon wafers or achieve specific functions.
Other applications of horizontal tube furnace in semiconductor manufacturing
Metalization process
Metalization process is one of the important steps in semiconductor manufacturing, used to form metal electrodes or wires on silicon wafers. Horizntal tube furnaces can be used for annealing treatment in metallization processes to improve the adhesion and stability of metal electrodes or wires.
During the annealing process, the metalized silicon wafer is placed in the furnace chamber of a horizntal tube furnace and kept at high temperature for a period of time to make the bonding between the metal electrode or wire and the silicon wafer tighter, thereby improving its adhesion and stability.
Etching process
Etching process is a step used in semiconductor manufacturing to remove excess material from the surface of silicon wafers. A horizntal tube furnace can be used for annealing treatment after etching process to remove damage and stress generated during the etching process.
During the annealing process, the etched silicon wafer is placed inside a horizntal tube furnace and kept at high temperature for a period of time, gradually releasing the internal stress of the silicon wafer and rearranging the lattice, thereby removing the damage and stress generated during the etching process.
Packaging process
The packaging process is the final step in semiconductor manufacturing, used to encapsulate semiconductor devices within protective shells to improve their reliability and stability. A horizntal tube furnace can be used for annealing treatment in packaging processes to remove stress and damage generated during the packaging process.
During the annealing process, the packaged semiconductor device is placed inside a horizntal tube furnace and kept at high temperature for a period of time to gradually release the stress inside the packaging material, rearrange the lattice, and remove the stress and damage generated during the packaging process.
Reduce exhaust temperature-Improve thermal efficiency
Optimized convection section design

Increase the number of convection tubes
By increasing the number of convection tubes, the contact area between the flue gas and the heating surface can be expanded, so as to improve the heat exchange efficiency and reduce the exhaust temperature.
Optimized convection tube arrangement
Reasonable arrangement of convection tube makes it more effective to capture and transfer the heat of flue gas. For example, staggered layout or spiral layout can be used to increase the flow path and residence time of smoke in the pipe.

Improve the heating surface efficiency
Use efficient heat transfer materials
Select materials with high thermal conductivity to make heating surfaces, such as stainless steel, copper alloy, etc., to improve heat exchange efficiency.
Keep the heating surface clean
Regularly clean the dust and dirt on the heating surface and keep its surface clean to improve the heat transfer efficiency. Dust accumulation and dirt will reduce the heat transfer performance of the heating surface, resulting in an increase in exhaust temperature.
Adjust the combustion process
Reasonable control of excess air coefficient
The air excess coefficient is the ratio of the actual air supply to the theoretical air supply. Reasonable control of excess air coefficient, avoid too much air into the furnace, can reduce the smoke volume, thereby reducing the exhaust temperature.
Improve fuel combustion efficiency
By optimizing the design of the burner and adjusting the combustion parameters, such as fuel injection speed and combustion chamber temperature, the combustion efficiency of the fuel can be improved, and the amount of incomplete combustion fuel can be reduced, thus reducing the exhaust temperature.
Increase waste heat recovery equipment
Install air preheater
The air preheater can use the waste heat of the flue gas to preheat the air entering the furnace, thereby improving the combustion efficiency and reducing the exhaust temperature.
Set up waste heat boiler
The waste heat boiler can recover the waste heat in the flue gas and convert it into useful energy such as steam or hot water, thereby reducing the exhaust temperature and improving energy utilization efficiency.
Other measures
Strengthen insulation measures
Good heat preservation treatment for the furnace body of horizontal tube furnace can reduce the heat loss and reduce the exhaust temperature.
Regular maintenance and maintenance
Regular maintenance and maintenance of the horizontal tube furnace, such as checking the heating surface, cleaning the ash, adjusting the combustion parameters, can ensure its normal operation and reduce the smoke exhaust temperature.
It should be noted that in the process of reducing the smoke exhaust temperature, factors such as the economy, safety and reliability of the equipment need to be considered comprehensively. At the same time, it is also necessary to choose the appropriate measures and methods according to the specific process requirements and operating conditions.
In addition, when the exhaust temperature is too low, it may cause low temperature dew point corrosion on the heat exchange surface. Therefore, when selecting the exhaust temperature, factors such as thermal efficiency and equipment life need to be weighed to ensure that the exhaust temperature can reduce heat loss without causing damage to the equipment.
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