Short Path Distillation Kit
(1)Flask:2L, 2x24/40 interfaces
(2)Receiving bottle:2x500mL,24/40 interface
(3)Cold trap:1L
2. 5L Short Path Distillation Kit:
(1)Flask:5L,34/45 interface,24/40 interface
(2)Receiving bottle:2x1000mL,24/40 interface
(3)Cold trap:1L
3. 10L Short Path Distillation Kit:
(1)Flask:10L,24/40 interface,2x34/45 interface
(2)Receiving bottle:2x2000mL,24/40 interface
(3)Cold trap:1L
4. 20L Short Path Distillation Kit:
(1)Flask:20L,24/40 interface,2x34/45 interface
(2)Receiving bottle:4x2000mL,24/40 interface
(3)Cold trap:2x1L
Description
Technical Parameters
The short-path distillation kit is a specialized liquid-liquid separation technology designed for efficient and precise distillation. It operates under high vacuum conditions, where the mean free path of vapor molecules exceeds the distance between the evaporation surface and the condensation surface. This kit utilizes the evaporation rates of various components in the feed liquid to achieve separation.
The short-path distillation kit offers numerous advantages such as low boiling points due to the negative pressure, short distances for vapor to condense, and minimal residual compounds after distillation. It finds applications in diverse industries, including fine chemicals, pharmaceuticals, food processing, and petroleum, for purifying and refining various materials.
We provide short-path distillation kit, please refer to the following website for detailed specifications and product information.
Product: https://www.achievechem.com/chemical-equipment/short-path-distillation-kit.html
Product Parameter
Short Path Distillation Kit Specification
The table will explain the details of equipment such as material, working voltage, stirring speed, heating power, interface size, etc
| No. | AC-SP2L | AC-SP5L | AC-SP10L | AC-SP20L | |
| Model | SP2L | SP5L | SP10L | SP20L | |
| Products |
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|
|
|
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| Material | Borosilicate glass 3.3 | ||||
| Heating temperature | 300℃ | ||||
| Working pressure | Approximately 5 Pa | ||||
| Distillation Flask | Volume(L) | 2 | 5 | 10 | 20 |
| Interface | 24/40 interfaces * 2 |
34/45 interface * 1 24/40 interface * 1 |
24/40 interface * 1 34/45 interface * 2 |
24/40 interface * 1 34/45 interface * 2 |
|
| Receiving Bottle | Volume(mL) | 500mL * 2 | 1000mL * 2 | 2000mL * 2 | 2000mL * 4 |
| Interface | 24/40 interface | 24/40 interface | 24/40 interface | 24/40 interface | |
| Cold Trap | Dry ice volume (L) | 1L | 1L | 1L | 1L * 2 |
| Heating jacket | Power(w) | 650 | 1100 | 2100 | 3000 |
| Mixing speed (rpm) | 50-1800 | ||||
| Motor power (w) | 40 | ||||
| Voltage | 220V 50/60Hz | ||||
| Vacuum Pump | Pumping rate (CFM) | 10 | 10 | 10 | 15 |
| Extraction rate | 2L/S | ||||
| Maximum vacuum degree | 0.06Pa | ||||
| Speed | 1400rpm | ||||
| Power | 370W | ||||
| Circulation Tank | Cooling temperature | -10℃ ~ 95℃ | |||
| Temperature accuracy | ± 0.01 ℃ | ||||
| Refrigeration power | 900W | ||||
| Heating power | 900W | ||||
| Circulating flow rate | 12L/min | ||||
Short Path Distillation Kit Content List
The types and quantities of equipment in the kit list.
| No. | AC-SP2L | AC-SP5L | AC-SP10L | AC-SP20L |
|---|---|---|---|---|
| Model | SP2L | SP5L | SP10L | SP20L |
| Products |
|
|
|
|
| Short range distillation head | 1 | 1 | 2 | 2 |
| Thermometer | 1 | 1 | 1 | 1 |
| Round bottom flask | 2L * 1 | 5L * 1 | 10L* 1 | 20L* 1 |
| Magnetic Stirring Electric Heating Mantle | 2L * 1 | 5L * 1 | 10L* 1 | 20L* 1 |
| Condenser Tube | 1 | 1 | 2 | 2 |
| Glass Belt Valve 3-way Joint | 1 | 1 | 2 | 2 |
| Vacuum Gauge | 1 | 1 | 2 | 2 |
| Stainless Steel Tee Joint | 1 | 1 | 2 | 2 |
| Cold Trap | 1 | 1 | 2 | 2 |
| Acceptance Bottle | 250ML * 2 | 1L * 2 |
2L * 2 500mL * 2 |
5L * 2 1L * 2 |
| Cork Flask Holder | 2 | 2 | 2 | 2 |
| Stainless Steel Lifting Platform | 1 | 2 | 2 | 2 |
| Iron Frame Platform | 1 | 0 | 2 | 2 |
| Chain Clamp | 1 | 1 | 2 | 2 |
| Vacuum Pump | 1 | 1 | 2 | 2 |
| Constant Temperature Circulation Tank | 1 | 1 | 1 | 1 |
Product Introduction
It includes essential components and apparatuses designed to facilitate the efficient separation and purification of liquid mixtures.
● Distillation Flask: This is a round-bottomed flask where the mixture to be distilled is initially placed. It is usually made of glass and has a standard socket joint for connecting other components.
● Heating Source: A heat source, such as a heating mantle or a heating bath, is used to provide controlled and uniform heating to the distillation flask. This allows the mixture to evaporate without reaching its boiling point.
● Condenser: The condenser consists of a glass tube or coil where the vapors generated in the distillation flask are cooled and condensed back into liquid form. It promotes the separation of volatile components from the mixture.
● Vacuum Pump: A vacuum pump is employed to create a reduced pressure environment within the distillation setup. Lowering the pressure lowers the boiling points of the compounds, allowing for distillation at lower temperatures and minimizing thermal degradation.
● Collection Flask: This flask is used to collect the purified distillate, which condenses after passing through the condenser. It is typically connected to the condenser outlet and is placed under vacuum.
Product Features
High vacuum, low distillation temperature, short residence time, high evaporation efficiency, continuous distillation process.
For the separation of high molecular weight, high boiling point, heat sensitivity and easy oxidation materials, high yield and better product quality can be obtained.
Short-distance distillation equipment can not only remove low-molecular-weight substances in liquid, such as organic solvents and odor, but also selectively distill out the target products and remove other impurities, so it is regarded as the protector and returner of natural quality.
Short-distance distillation equipment can realize the physical process that traditional separation methods can't, so it is widely used as a means of deodorization, decoloration and purification in the separation of some high-value materials.
The wall of short-distance distillation equipment is self-cleaning, with less pollution and easy cleaning.
Applications
Short path distillation kit is an efficient equipment for distilling and separating liquid mixtures. By shortening the distance between evaporation surface and condensation surface, light components can be quickly cooled after evaporation, thus achieving efficient separation. This kind of kit usually consists of glassware and heating device, which can be used in many fields.
Laboratory Research
In the laboratory, it can be used to separate and analyze liquid mixtures, such as organic solvents, chemical reagents and food additives.
Industrial Production
In industrial production, the glass short-path distillation kit can be used to separate and purify liquid mixtures, such as petroleum, chemical raw materials and pharmaceutical raw materials.
Wastewater Treatment
The kit can also be used for wastewater treatment, such as removing harmful substances such as organic matter and heavy metals from wastewater.
Food Processing
In food processing, glass short-path distillation kit can be used to extract and separate useful ingredients in food, such as vegetable oil and caffeine.
Precaution for Use
Before operation, the inlet and outlet valves of cooling water must be opened to check whether the pressure is within the normal range.
Before opening the inlet and outlet valves of each component coolant, it must be confirmed that the valves are in the correct open state.
During operation, direct contact with the surface of the external heating body of the equipment should be avoided to prevent burns.
In the process of distillation, we should pay attention to observe whether the ethanol in the low temperature and constant temperature tank is enough, and add ethanol in time.
After the operation, the inlet and outlet valves of cooling water and cooling liquid of each component shall be closed in time.
When using liquid nitrogen, we should pay attention to check whether the liquid nitrogen in the liquid nitrogen barrel is sufficient and replenish the liquid nitrogen in time.
When collecting distillation products with collecting bottles, the appropriate specifications of collecting bottles should be selected according to the boiling point differences of different components, and the products should be collected according to the marks.
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