Complete Short Path Distillation Kit
2. Capacity(L): 1-20
3. Applications: Chemical industry, pharmaceutical industry, flavor and fragrance industry, food and beverage industry, cannabis extract, etc.
4. Turnkey Solution: Heating and cooling circulator, vacuum pump
5. Manufacturer: ACHIEVE CHEM Xi’an Factory
6. 16 years experiences on Chemical Equipment
7. CE and ISO certification
8. Professional shipping
9. One-year worry-free warranty
10. 24/7 after-sales service
Description
Technical Parameters
A complete short path distillation kit is an indispensable tool for many industries that rely on precise separation processes. It has a series of components, including evaporator, condenser, receiving bottle, heating source, vacuum pump, controller, cold trap, and special glassware, which can efficiently extract and purify compounds. A complete short-range ditillation kit is an indispensable precision tool in scientific research and industrial production. It integrates numerous components such as evaporator, condenser, receiving bottle, heating source, vacuum pump, controller, cold trap, and special glassware. Through intelligent control and efficient collaborative operation, it achieves precise and efficient compound extraction and purification. With the continuous advancement and innovation of technology, short-range ditillation technology will demonstrate its unique charm and value in more fields. Short range ditillation is an effective method for separating complex mixtures into their constituent chemical components. The core of this process is the ditillation kit, which is a complex professional equipment component designed to achieve efficient and precise separation.
Product Introduction
Short-path ditillation kit is a special liquid-liquid separation technology, which is different from traditional ditillation technology by relying on the principle of boiling point difference, but by using the difference of average free paths of different substances. In the complete short path distillation kit, the steps to realize liquid-liquid separation are as follows:
1.
The liquid mixture to be separated is continuously and uniformly fed into the kit from the feeding unit.
2.
The liquid mixture flows along the heating plate and is heated, and light and heavy molecules will escape from the liquid surface and enter the gas phase.
3.
Because the free paths of light and heavy molecules are different, light molecules reach the condensation plate and are condensed and discharged, while heavy molecules cannot reach the condensation plate and are discharged along the mixed liquid.
4.
The collector discharges the liquid mixture collected in the condenser from the kit and collects it in a suitable container.
Specifications
Product Introduction
components
Feeding unit:
Like the "mother" in the family, it plays a "role" in taking care of the whole family, constantly preparing various "ingredients" (liquid mixture to be separated) to provide a foundation for the next separation process.
Evaporator:
Just like the "father" in the family, it is responsible for converting the "food" prepared by "mother" into a gas state. This step is the core of the whole family ditillation process, heating the "food" to a proper temperature and forming gas.
Condenser:
Just like the "grandfather" in the family, after the "father" heats the "food", he is responsible for cooling and collecting it, and converting the "food" in gas state into liquid state again.
Collector:
Like the "grandma" in the family, it is responsible for sorting out the liquid "ingredients" collected by "grandpa", discharging the kit and collecting them in appropriate containers to prepare for the next cooking or use.
Heating unit:
It can be compared to the "kitchen" in the family, which provides a heat source for the whole ditillation process, so that "Dad" can heat the "food" and convert it into gas.
Vacuum system:
Like the "ventilation system" in the family, the steam formed after "Dad" is heated is quickly exhausted by vacuuming, creating a more pure environment for the next ditillation process.
|
|
|
Process conditions for vacuum distillation
The following will take the industrial preparation of sponge zirconium as an example to explain the process conditions of complete short path distillation kit.
Equipment structure
Generally, a bottom cooled vacuum ditillation furnace is used, as shown in the figure "Vacuum Ditillation Furnace". The magnesium crucible is placed upside down on the support, and most of the melted magnesium flows down into the salt tank at high temperatures. After the melted magnesium flows out of the crucible, the capillary pores inside the zirconium sponge can be exposed, thereby increasing the evaporation area and speed, and shortening the ditillation cycle.
01
Distilled material batch
The ditillation rate is related to the amount of distilled material. As the amount of material increases, as long as the vacuum system is properly configured, including mechanical pumps, booster pumps, diffusion pumps, and has sufficient exhaust rate, the ditillation time does not increase proportionally, but is appropriately extended to obtain the same product quality.
02
Distilled temperature
Although the higher the temperature, the faster the volatilization rate, in order to prevent the formation of alloys (eutectic temperature: 935 ℃), the ditillation temperature should be controlled at a maximum of around 900 ℃.
03
Vacuum degree
High vacuum degree is beneficial for the evaporation of magnesium and the reduction of gas pollution. In the vacuum ditillation process, it is required that the vacuum degree in the later stage should not exceed 0.013Pa.
04
Cooling water temperature
There is a water-cooled jacket at the bottom of the ditillation tank. The amount of cooling water should be appropriate to ensure good condensation efficiency. The temperature of the cooling water is controlled between 35-50 ℃.
05
Applications
The following steps are required to extract rose essential oil with a short path ditillation kit:
Preparation materials: Collect fresh rose petals and clean them. Make sure to choose organic rose petals without pesticide residues to obtain high-quality essential oil.
Filling the evaporator: Put the washed rose petals evenly in the flower basket or filter bag of the evaporator. Make sure not to overfill, so that steam can be extracted smoothly through the petals.
Connecting the condenser: Connect the evaporator with the condenser and the collection container. Ensure tight connection to prevent steam leakage.
Turn on the heating source and vacuum pump: Turn on the heating source to provide an appropriate temperature, generally 80-100 degrees Celsius. Start the vacuum pump to create an appropriate vacuum environment.
Start extraction: With the heating and vacuum operation, the rose petals in the evaporator begin to release volatile components and form steam. When the steam passes through the condenser, it will cool and turn into liquid, that is, rose essential oil.
Collect essential oil: The extracted rose essential oil will gradually accumulate in the collection container. According to the need, the collection container can be changed regularly to collect essential oil in batches.
Obtain higher purity essential oil (optional): If higher purity rose essential oil is needed, it can be extracted several times or further refined and purified by other technologies.
|
|
|
Essential oils are highly concentrated, aromatic extracts derived from various plant parts such as leaves, flowers, bark, roots, and fruits. These oils capture the essence of the plant they originate from, encapsulating its unique scent and therapeutic properties. Extracted through methods like steam distillation, water distillation, or hydro-distillation, essential oils are known for their potent and diverse benefits.
Used widely in aromatherapy, essential oils can evoke emotional responses, promote relaxation, and enhance overall well-being. Their natural compounds have antibacterial, antiviral, and antifungal properties, making them effective in supporting immune health and skin care. For instance, lavender oil is renowned for its calming effects and ability to aid sleep, while tea tree oil is valued for its powerful antiseptic qualities.
Essential oils can be utilized in various ways, including diffusion, topical application, and even ingestion (in small, diluted amounts and under expert guidance). When incorporated into skincare products, cleaning solutions, or personal care routines, they offer a natural and holistic alternative to synthetic fragrances and chemicals.
In summary, essential oils are more than just fragrant oils; they are powerful natural remedies that can support physical, mental, and emotional health. Their versatility and efficacy make them a staple in holistic health practices and natural living lifestyles.
Simple device
The complete short path distillation kit is a comprehensive, all-in-one solution designed for researchers, laboratories, and enthusiasts engaged in the precise distillation of various chemicals and compounds. This kit offers a streamlined approach to short path distillation, a technique known for its efficiency in separating high-purity compounds from mixtures, especially those with low volatility or heat sensitivity.
The kit includes a robust glass still equipped with a short path condenser, which minimizes the distance vapor travels, reducing the likelihood of condensation-induced contamination and heat loss. This feature ensures higher yields and purer products. It also boasts a vacuum pump system to create a low-pressure environment, further lowering distillation temperatures and protecting sensitive materials.
Additional components such as a heating mantle, temperature controller, and collection flask are integrated to provide a seamless distillation workflow. The heating mantle ensures uniform and controlled heating, while the temperature controller allows for precise adjustments, enhancing reproducibility. The collection flask safely captures the distilled product, maintaining its purity until further use.
The complete short path distillation kit is characterized by its ease of use, durability, and versatility. Suitable for a wide range of applications, from pharmaceutical research to essential oil extraction, it represents a valuable addition to any laboratory seeking high-quality distillation results. Its compact design and modular components make it an ideal choice for both small-scale experiments and larger-scale operations, offering a balance of performance and convenience.
Hot Tags: complete short path distillation kit, China complete short path distillation kit manufacturers, suppliers, factory, Rotovap Machine, Single Layer Glass Reactor, Short Path Molecular Distillation, Double Glass Reactor, Teflon Autoclave, Molecular Distillation Equipment
Send Inquiry
